HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl formate → N-formyl-4-(3-azidopropyl)-piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl formate | HCID 7865 | — |
| Reactant | 4-(3'-Azidopropyl)-piperidine | HCID 13503220 | — |
| Product | N-formyl-4-(3-azidopropyl)-piperidine | HCID 13503223 | — |
Reaction Steps
A solution of 4-(3'-azidopropyl)-piperidine (1.5 g) in methyl formate (5 ml) was refluxed for 1 hour. Evaporation to dryness gave the desired compound as an oil. The IR-spectrum (CHCl3) showed strong bands at 2100, 1660, 1440 and 1270 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04345071 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-78226627656b46d0aa0bbec9bf151a48 |
| Source note | uspto-grants-1982_08 |