Ethanol → HCID 20528725, compound

HRID 67173Notes

Reaction equation

HRID 67173 reaction equation
Cl[C:2]([CH:4]1[CH2:11][CH:10]2[CH2:12][CH:6]([C:7](=[O:14])[NH:8][C:9]2=[O:13])[CH2:5]1)=[O:3].[CH2:15]([OH:17])[CH3:16]>>[C:2]([CH:4]1[CH2:11][CH:10]2[CH2:12][CH:6]([C:7](=[O:14])[NH:8][C:9]2=[O:13])[CH2:5]1)([O:17][CH2:15][CH3:16])=[O:3]

Participants

3

Reactant 2

HCID 702EthanolHCID 20528705HCID 20528705, compound

Product 1

HCID 20528725HCID 20528725, compound

Procedure

A mixture of 7-chlorocarbonyl-3-azabicyclo[3.3.1]nonane-2,4-dione (2 g) and absolute ethanol (25 ml) was left overnight at room temperature and evaporated to leave the desired compound which was used in the next step without purification.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-68eb4f56430a45d3834859058d458faa
Source dataset
uspto-grants-1982_08
Patent number
US04345071

Reaction notes

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