HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-benzyloxy-3-methyl-2,3,4,9-tetrahydro-1H-beta-carboline → HCID 22018508, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-benzyloxy-3-methyl-2,3,4,9-tetrahydro-1H-beta-carboline | HCID 22018514 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22018508 | HCID 22018508 | 72.3% |
Reaction Steps
A solution of 6-benzyloxy-3-methyl-2,3,4,9-tetrahydro-1H-β-carboline (60 mg) in ethanol (4 mL) was added to a suspension of 10% Pd/C (100 mg) in ethanol (10 mL). The mixture was stirred at rt for 16 h under an atmosphere of hydrogen. The mixture was filtered through celite and evaporation of the filtrate yielded 3-methyl-2,3,4,9-tetrahydro-1H-β-carbolin-6-ol (30 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07084154B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-6e073a3a3c75488e81aeb22ebd875f71 |
| Source note | uspto-grants-2006_08 |