HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetoacetate → 1-(9-Octadecenyl)-4-methyl-3,6,7,8-tetrahydro-1,5-diazocin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | N-(9-octadecenyl)-1,3-propylenediamine | HCID 40764 | — |
| Product | 1-(9-Octadecenyl)-4-methyl-3,6,7,8-tetrahydro-1,5-diazocin-2-one | HCID 53794468 | — |
Reaction Steps
Into an apparatus similar to that in Example 1, were charged 324.1 g (1 mole) of N-(9-octadecenyl)-1,3-propylenediamine and 130.1 g (1 mole) of ethyl acetoacetate. At 110° to 120° C. and under a reduced pressure of 50 mmHg, 18 g of water and 46 g of ethanol had been distilled off to obtain 1-(9-octadecenyl)-4-methyl-3,6,7,8-tetrahydro-1,5-diazocin-2-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346087 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-76e1e52fc15e4065923719a1818bf2bd |
| Source note | uspto-grants-1982_08 |