HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetoacetate → HCID 20527085, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | N~1~-Hexadecylethane-1,2-diamine | HCID 13052964 | — |
| Product | HCID 20527085 | HCID 20527085 | — |
Reaction Steps
Into an apparatus similar to that in Example 1, were charged 284.1 g (1 mole) of N-hexadecylethylenediamine and 130.1 g (1 mole) of ethyl acetoacetate. At 160° to 170° C., 18 g of water and 46 g of ethanol were distilled off to obtain 4-hexadecyl-7-methyl-3,6-dihydro-2H-1,4-diazepin-5-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346087 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-2ade61607eb14e5897f05b62ab572e59 |
| Source note | uspto-grants-1982_08 |