HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-dodecylethylenediamine → 4-dodecyl-6-methyl-3,6-dihydro-2H-1,4-diazepin-5-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-dodecylethylenediamine | HCID 10561362 | — |
| Reactant | Ethyl 2-Formylpropionate | HCID 10898741 | — |
| Product | 4-dodecyl-6-methyl-3,6-dihydro-2H-1,4-diazepin-5-one | HCID 20527043 | — |
Reaction Steps
Into an apparatus similar to that in Example 1, were charged 228.1 g (1 mole) of N-dodecylethylenediamine and 130.1 g (1 mole) of ethyl 2-formylpropionate. At 140° to 145° C., 18 g of water and 46 g of ethanol were distilled off to obtain 4-dodecyl-6-methyl-3,6-dihydro-2H-1,4-diazepin-5-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346087 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-4afd6959548e48daabbc02c6e62ec71d |
| Source note | uspto-grants-1982_08 |