HRID67759

反应详情

EQUATION

反应方程式

HRID 67759 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Obtained by a procedure analogous to that indicated in Example 1 (b), from 4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-(2,3-dimethylphenyl-imino)thiazolidin-4-ol hydrobromide, by boiling in glacial acetic acid for 2 hours and filtering off the crystals at room temperature. Colorless crystals from glacial acetic acid; melting point 256° C. (with decomposition).

WORKUP

后处理

  1. customObtained by a procedure analogous to
  2. filtrationfiltering off the crystals at room temperature