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HRID67764

反应详情

EQUATION

反应方程式

HRID 67764 的结构方程式

REACTANTS

反应物

1
结构：Br.COc1cc(N=C2SCC(O)(c3ccc(Cl)c(S(=O)(=O)N(C)C)c3)N2C)cc(OC)c1OC
HCID70531920

未命名化合物

PRODUCTS

生成物

1
结构：Br.COc1cc(N=c2scc(-c3ccc(Cl)c(S(=O)(=O)N(C)C)c3)n2C)cc(OC)c1OC
HCID20527262

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

Obtained by a procedure analogous to that indicated in Example 1(b), from 4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-(3,4,5-trimethoxyphenyl-imino)-thiazolidin-4-ol hydrobromide, by boiling for 30 minutes in glacial acetic acid and precipitating with diisopropyl ether. Melting point 246° C.

WORKUP

后处理

  1. customObtained by a procedure analogous to
  2. customprecipitating with diisopropyl ether