1-Hexyl-3-phenyl-2-thiourea → HCID 20527333, compound

HRID 67766Notes

Reaction equation

HRID 67766 reaction equation
[Br:1]CC(C1C=CC(Cl)=C(S(=O)(=O)N(C)C)C=1)=O.C(NC(=S)NC1C=CC=CC=1)CCCCC.Br.[Cl:35][C:36]1[CH:41]=[CH:40][C:39]([C:42]2(O)[CH2:46][S:45][C:44](=[N:47][C:48]3[CH:53]=[CH:52][CH:51]=[CH:50][CH:49]=3)[N:43]2[CH2:54][CH2:55][CH2:56][CH2:57][CH2:58][CH3:59])=[CH:38][C:37]=1[S:61](=[O:66])(=[O:65])[N:62]([CH3:64])[CH3:63]>>[BrH:1].[Cl:35][C:36]1[CH:41]=[CH:40][C:39]([C:42]2[N:43]([CH2:54][CH2:55][CH2:56][CH2:57][CH2:58][CH3:59])[C:44](=[N:47][C:48]3[CH:49]=[CH:50][CH:51]=[CH:52][CH:53]=3)[S:45][CH:46]=2)=[CH:38][C:37]=1[S:61](=[O:66])(=[O:65])[N:62]([CH3:64])[CH3:63]

Participants

4

Reactant 3

HCID 27592821-Hexyl-3-phenyl-2-thioureaHCID 204768462-Bromo-4'-chloro-3'-dimethylsulfamoylacetophenoneHCID 20527381HCID 20527381, compound

Product 1

HCID 20527333HCID 20527333, compound

Procedure

Obtained (a) by a procedure analogous to that indicated in Example 1(a), from 2-bromo-4'-chloro-3'-dimethylsulfamoylacetophenone and 3-n-hexyl-1-phenylthiourea, or (b) by a procedure analogous to that indicated in Example 1(b), from 4-(4-chloro-3-dimethylsulfamoylphenyl)-3-n-hexyl-2-phenyliminothiazolidin-4-ol hydrobromide. Colorless crystals; melting point 234° C. (with decomposition).

Sources & evidence

ORD record
ord-bbc3cd6ef51c4d75a58137ce9fca5d23
Source dataset
uspto-grants-1982_08
Patent number
US04346088

Reaction notes

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