Urea, 1-butyl-3-phenyl-2-thio- → HCID 20527180, compound

HRID 67767Notes

Reaction equation

HRID 67767 reaction equation
C(NC(=S)NC1C=CC=CC=1)CCC.[Br:15]CC(C1C=CC(Cl)=C(S(=O)(=O)N(C)C)C=1)=O.Br.[CH2:33]([N:37]1[C:41]([C:43]2[CH:48]=[CH:47][C:46]([Cl:49])=[C:45]([S:50](=[O:55])(=[O:54])[N:51]([CH3:53])[CH3:52])[CH:44]=2)(O)[CH2:40][S:39][C:38]1=[N:56][C:57]1[CH:62]=[CH:61][CH:60]=[CH:59][C:58]=1[CH3:63])[CH2:34][CH2:35][CH3:36]>>[BrH:15].[CH2:33]([N:37]1[C:41]([C:43]2[CH:48]=[CH:47][C:46]([Cl:49])=[C:45]([S:50](=[O:54])(=[O:55])[N:51]([CH3:53])[CH3:52])[CH:44]=2)=[CH:40][S:39][C:38]1=[N:56][C:57]1[CH:62]=[CH:61][CH:60]=[CH:59][C:58]=1[CH3:63])[CH2:34][CH2:35][CH3:36]

Participants

4

Reactant 3

HCID 3034183Urea, 1-butyl-3-phenyl-2-thio-HCID 204768462-Bromo-4'-chloro-3'-dimethylsulfamoylacetophenoneHCID 20527351HCID 20527351, compound

Product 1

HCID 20527180HCID 20527180, compound

Procedure

Obtained (a) by a procedure analogous to that indicated in Example 1(a), from 3-n-butyl-1-phenylthiourea and 2-bromo-4'-chloro-3'-dimethylsulfamoylacetophenone, or (b) from 3-n-butyl-4-(4-chloro-3-dimethylsulfamoylphenyl)-2-(2-methylphenyl-imino)-thiazolidin-4-ol hydrobromide. Colorless crystals; melting point 238° C.

Sources & evidence

ORD record
ord-0cc7fdb0422e4629bf0765f8f8634d7a
Source dataset
uspto-grants-1982_08
Patent number
US04346088

Reaction notes

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