HRID67769

反应详情

EQUATION

反应方程式

HRID 67769 的结构方程式

PROCEDURE

实验过程

Obtained by a procedure analogous to that indicated in Example 1(b), from 4-(4-chloro-3-dipropylsulfamoylphenyl)-3-methyl-2-(2-methylphenyl)-thiazolidin-4-ol hydrobromide, by boiling in glacial acetic acid for 2 hours. The reaction mixture is concentrated, water is added to the residue and the crystals are filtered off. Melting point 218°-220° C.

WORKUP

后处理

  1. customObtained by a procedure analogous to
  2. concentrationThe reaction mixture is concentrated
  3. additionwater is added to the residue
  4. filtrationthe crystals are filtered off