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HRID67771

反应详情

EQUATION

反应方程式

HRID 67771 的结构方程式

REACTANTS

反应物

1
结构：Br.CCCN(CCC)S(=O)(=O)c1cc(C2(O)CSC(=Nc3cccc(C)c3C)N2C)ccc1Cl
HCID70532027

未命名化合物

PRODUCTS

生成物

1
结构：Br.CCCN(CCC)S(=O)(=O)c1cc(-c2csc(=Nc3cccc(C)c3C)n2C)ccc1Cl
HCID20527307

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

Obtained by a procedure analogous to that indicated in Example 1(b), from 4-(4-chloro-3-dipropylsulfamoylphenyl)-3-methyl-2-(2,3-dimethylphenyl-imino)thiazolidin-4-ol hydrobromide by refluxing in glacial acetic acid, subsequently evaporating and crystallizing the viscous residue under water. Colorless crystals from methanol/ether; melting point 210°-212°.

WORKUP

后处理

  1. customObtained by a procedure analogous to
  2. customsubsequently evaporating
  3. customcrystallizing the viscous residue under water