HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sarcosine → 1-Methyl-3-n-nonyl hydantoin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sarcosine | HCID 1088 | — |
| Reactant | Hydantoin | HCID 10006 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | capric N-chloramide | HCID 19040089 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | tert-Butanol | HCID 6386 | — |
| Product | 1-Methyl-3-n-nonyl hydantoin | HCID 70549405 | 90% |
Reaction Steps
In accordance with the procedure described in Example 6, 41 g (0.2 mol) capric N-chloramide were reacted with sarcosine, sodium hydroxide in a mixture of tertiary butanol and water and then processed. The hydantoin remained in the aqueous solution was an oil, that was extracted with ether. The ether was removed by distillation to yield 43 g (90% yield) 1-methyl-3-n-nonyl hydantoin of the formula ##STR10## having the following analysis:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346233 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-37b99b25d34c4e0887d8172c6d4f7e0f |
| Source note | uspto-grants-1982_08 |