Ethylenediamine → HCID 178433308, compound

HRID 67911Notes

Reaction equation

HRID 67911 reaction equation
[C:1]([NH:3][C:4](=[N:7][CH2:8][CH2:9][S:10][CH2:11][C:12]1[NH:16][CH:15]=[N:14][C:13]=1[CH3:17])SC)#[N:2].[CH2:18]([NH2:21])[CH2:19][NH2:20]>>[C:1]([NH:3][C:4]([NH:20][CH2:19][CH2:18][NH2:21])=[N:7][CH2:8][CH2:9][S:10][CH2:11][C:12]1[NH:16][CH:15]=[N:14][C:13]=1[CH3:17])#[N:2]

Participants

3

Reactant 2

HCID 3301EthylenediamineHCID 178503877HCID 178503877, compound

Product 1

HCID 178433308HCID 178433308, compound

Procedure

Reaction of N-cyano-N'-[2-((4-methyl-5-imidazolyl)methylthio)ethyl]-S-methylisothiourea with excess ethylenediamine at room temperature afforded the title compound m.p. 164°-167° (from acetonitrile-ethanol)

Sources & evidence

ORD record
ord-dc79c9978d1041da9cc45bce3ffcc126
Source dataset
uspto-grants-1982_08
Patent number
US04347250

Reaction notes

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