HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → HCID 53818980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | HCID 115309 | HCID 115309 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 53818980 | HCID 53818980 | — |
Reaction Steps
Iodine is added to a solution of 100 g of potassium iodide in 500 ml of water to saturation. This saturated solution is added dropwise to a solution of α-mercapto-β-(2-furyl)acrylic acid in 500 ml of acetonitrile and 30 ml of water until the color of iodine persists. The crude product which precipitates is recrystallized from methanol. M.P. 215° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04347255 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-6bd3178a9e0148e988dd79dc3763aed5 |
| Source note | uspto-grants-1982_08 |