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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 68182생성일: 2026년 10월 25일

Adipic Acid → Urethane acrylate

https://huagongshe.com/reaction/68182

반응식

참여 물질

역할이름HCID투입량
반응물Adipic AcidHCID 196—
반응물4-MethoxyphenolHCID 9015—
반응물2-Hydroxyethyl acrylateHCID 13165—
반응물Neopentyl glycolHCID 31344—
반응물2,6-Di-tert-butyl-4-methylphenolHCID 31404—
반응물IsocyanateHCID 105034—
반응물Isophorone diisocyanateHCID 169132—
반응물Cesium acetateHCID 5152919—
용매EthanolHCID 702—
생성물Urethane acrylateHCID 21863578—

반응 조건

온도50 °C

반응 단계

672.0 g of a polyester of adipic acid and neopentyl glycol with an OH number of about 200, 140.0 g of hydroxyethyl acrylate, 0.6 g of hydroquinone monomethyl ether, 1.21 g of 2,6-di-tert-butyl-4-methylphenol, 0.12 g of cesium acetate were initially introduced into a round-bottomed flask and heated to 50° C. 400.0 g of isophorone diisocyanate were then added dropwise over the course of 30 minutes. The mixture was left to react for a further 7 hours at 90-95° C., during which the NCO content dropped to 0.56%. The mixture was cooled to 60° C., then 520.0 g of ethanol were added and the mixture was left to react further for about 2 hours at 65-70° C. until the isocyanate content (NCO value) had dropped to 0. The resulting resin was filtered over a 50 μm filter and bottled.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08821841B2
출처 데이터셋uspto-grants-2014_09
ORD IDord-e11022da67c7404caadfbb5793860415
출처 메모uspto-grants-2014_09