HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[(4-Methylamino-3-nitro-benzoyl)-phenyl-amino]propionic acid methyl ester → 3-[(3-Amino-4-methylamino-benzoyl)-phenyl-amino]propionic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[(4-Methylamino-3-nitro-benzoyl)-phenyl-amino]propionic acid methyl ester | HCID 58069421 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-[(3-Amino-4-methylamino-benzoyl)-phenyl-amino]propionic acid methyl ester | HCID 18412336 | — |
Reaction Steps
The nitro group of product 1a was reduced by hydrogenation at room temperature in ethanol with Pd (10% on charcoal) as catalyst.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08821871B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-58567c32622f4b2a9ffc9a6fe55bc69b |
| Source note | uspto-grants-2014_09 |