HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 10-methylacridinium-9-carboxylate trifluoromethanesulfonate → Methyl 10-methylacridan-9-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 10-methylacridinium-9-carboxylate trifluoromethanesulfonate | HCID 86648905 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 10-methylacridan-9-carboxylate | HCID 12813956 | — |
Reaction Steps
A solution of methyl 10-methylacridinium-9-carboxylate trifluoromethanesulfonate (75), 4.25 parts, in methanol is reduced as described in Example I to give 3.2 parts of methyl 10-methylacridan-9-carboxylate and the isolated product has the following structure confirmed by NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08822233B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-e520dbfed13343b78f1b05d43e37b7af |
| Source note | uspto-grants-2014_09 |