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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 68356Generated: October 28, 2026

Trifluoroacetic acid → HCID 131731809, compound

https://huagongshe.com/reaction/68356

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 131731810HCID 131731810—
SolventDichloromethaneHCID 6344—
ProductHCID 131731809HCID 13173180979%

Reaction Steps

By using the procedure described in Step-4 of Example-1 above, and by using tetrabutylammonium salt of trans-3-[N′-(6-sulfooxy-7-oxo-1,6-diaza-bicyclo[3.2.1]octane-2-carbonyl)-hydrazinocarbonyl]-(R)-piperidin-1-carboxylic acid tert-butyl ester (24 gm, 0.032 mmol), dichloromethane (60 ml) and trifluoroacetic acid (60 nil) to provide the title compound in 10 gm quantity as a white solid, in 79% yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08822450B2
Source datasetuspto-grants-2014_09
ORD IDord-91b0d2104b5442869f2df4f36f513e22
Source noteuspto-grants-2014_09