Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → 1-methyl-1H-benzo[d]imidazole-6-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Methylamine | HCID 6329 | — |
| 반응물 | Methyl 3-fluoro-4-nitrobenzoate | HCID 592761 | — |
| 생성물 | 1-methyl-1H-benzo[d]imidazole-6-carbaldehyde | HCID 22464914 | — |
반응 단계
The title compound was synthesized in a similar manner as described for intermediate J using methyl amine solution in MeOH instead of 2-pyrrolidin-1-yl-ethylamine to react with 3-fluoro-4-nitro-benzoic acid methyl ester (xiv) (tR 1.56 min (conditions 8), MH+=161).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08822468B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-26a1f4814fb04860a5675fe1a3ebcce0 |
| 출처 메모 | uspto-grants-2014_09 |