HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzyl-4-piperidone → 1-Benzyl-4-methylpiperidin-4-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzyl-4-piperidone | HCID 19220 | — |
| Reactant | HCID 178418348 | HCID 178418348 | — |
| Product | 1-Benzyl-4-methylpiperidin-4-ol | HCID 10845913 | — |
Reaction Steps
1-Benzyl-piperidin-4-one was reacted with methyllithium according to Method AI and the 1-benzyl-4-methyl-piperidin-4-ol obtained was hydrogenated in debenzylating conditions according to Method AH. In this way the product was obtained with molecular weight 115.1 (C6H13NO); MS (ESI): 116 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08822495B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-95707ea0463f418f87866a7d892da643 |
| Source note | uspto-grants-2014_09 |