3-Methoxypropylamine → HCID 178495292, compound

HRID 69785Notes

Reaction equation

HRID 69785 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][CH2:5][NH2:6].[OH:7][N:8]=[C:9]([C:11]1[C:15]([NH:16]CCCOC)=[N:14][O:13][N:12]=1)N>>[NH2:16][C:15]1[C:11]([C:9](=[N:8][OH:7])[NH:6][CH2:5][CH2:4][CH2:3][O:2][CH3:1])=[N:12][O:13][N:14]=1

Participants

3

Reactant 2

HCID 16723-MethoxypropylamineHCID 136367781HCID 136367781, compound

Product 1

HCID 178495292HCID 178495292, compoundYield 93%

Procedure

The desired compound was prepared according to the procedure of Example 1, step C, using 3-methoxy-1-propanamine as the starting material in 93% yield. LCMS for C7H14N5O3 (M+H)+: m/z=216.1. Step B: N′-Hydroxy-4-[(3-methoxypropyl)amino]-1,2,5-oxadiazole-3-carboximidamide

Sources & evidence

ORD record
ord-e2c108ee964046c582511e1641d6a512
Source dataset
uspto-grants-2014_09
Patent number
US08822511B2

Reaction notes

Loading…