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HRID69920

反应详情

EQUATION

反应方程式

HRID 69920 的结构方程式

REACTANTS

反应物

2
结构：Nc1ccc(Br)nc1C(=O)O
HCID45480452

3-Amino-6-bromopyridine-2-carboxylic acid

C6H5BrN2O2

结构：CC(C)(C)c1nccc(N2CCCC(O[Si](C)(C)C(C)(C)C)C2)c1N
HCID86669190

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)[Si](C)(C)OC1CCCN(c2ccncc2NC(=O)c2nc(Br)ccc2N)C1
HCID86669192

未命名化合物

PROCEDURE

实验过程

Following Method 11 of Example 305, tert-butyl (+/−)-4-(3-(tert-butyldimethylsilyloxy)piperidin-1-yl)pyridin-3-amine was coupled to 3-amino-6-bromopicolinic acid yielding 3-amino-6-bromo-N-(4-(3-(tert-butyldimethylsilyloxy)-piperidin-1-yl)pyridin-3-yl)picolinamide. LCMS (m/z): 506.2 (MH+); LC Rt=4.03 min.