4-Chlorobenzenesulfonamide → HCID 14536794, compound

HRID 703147Notes

Reaction equation

HRID 703147 reaction equation
Br[CH2:2][CH2:3][S:4][CH2:5][CH2:6][CH2:7][C:8]([CH3:15])([CH3:14])[C:9]([O:11][CH2:12][CH3:13])=[O:10].[Cl:16][C:17]1[CH:22]=[CH:21][C:20]([S:23]([NH2:26])(=[O:25])=[O:24])=[CH:19][CH:18]=1>>[Cl:16][C:17]1[CH:18]=[CH:19][C:20]([S:23]([NH:26][CH2:2][CH2:3][S:4][CH2:5][CH2:6][CH2:7][C:8]([CH3:15])([CH3:14])[C:9]([O:11][CH2:12][CH3:13])=[O:10])(=[O:24])=[O:25])=[CH:21][CH:22]=1

Participants

3

Reactant 2

HCID 668244-ChlorobenzenesulfonamideHCID 14536793HCID 14536793, compound

Product 1

HCID 14536794HCID 14536794, compoundYield 63%

Procedure

from ethyl 8-bromo-2,2-dimethyl-6-thiaoctanoate and 4-chlorobenzenesulphonamide; yield 63% of theory; colourless oil;

Sources & evidence

ORD record
ord-d3599036dfb946bc88899ade6a6a0f21
Source dataset
uspto-grants-1991_01
Patent number
US04981873

Reaction notes

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