HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 15616401, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | Quinuclidine, 3-amino-, dihydrochloride | HCID 197853 | — |
| Reactant | Maleate(2-) | HCID 5288227 | — |
| Reactant | N-Carbamoyl-4-methoxybenzamide | HCID 12757374 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 15616401 | HCID 15616401 | — |
Reaction Steps
The above compound was prepared, following the procedure of Example 14b, from 3-aminoquinuclidine dihydrochloride (1.0 g, 5 mmol), 4-methoxybenzoylurea (0.97 g, 5 mmol) and di-isopropylethylamine (1.29 g, 10 mmol) in pyridine (20 ml). The product (1.12 g) was converted to 1:1 maleate half hydrate, mp 166°-168° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04983600 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-cd1cc0ddcb664575ad8d34948d9f190b |
| Source note | uspto-grants-1991_01 |