HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → HCID 287116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 3-Ethylpyridine-2-carboxylic acid | HCID 17841857 | — |
| Solvent | Ammonia | HCID 222 | — |
| Product | HCID 287116 | HCID 287116 | — |
Reaction Steps
A mixture of sodium (0.23 g, 10 mmol), urea (0.8 g, 13.3 mmol) and liquid ammonia (40 ml) was stirred until the blue colour was discharged, then ethyl 2-pyridinecarboxylic acid (2.85 g, 18.8 mmol) was added all at once. After 1 h the ammonia was evaporated and the residue triturated with water to give the above compound, mp 183°-185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04983600 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-3e0b9a596cdb4a36901c358a1ff6512f |
| Source note | uspto-grants-1991_01 |