HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 703469Generated: October 30, 2026
N-methyl-2-pyrrolidone → HCID 15158253, compound
https://huagongshe.com/reaction/703469
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Reactant | 4,6-Dichloropyrimidine | HCID 70943 | — |
| Reactant | 9H-carbazol-9-amine | HCID 276207 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 15158253 | HCID 15158253 | — |
Reaction Steps
To 150 ml of 1-methyl-2-pyrrolidinone was added 10.0 g of 9H-carbazol-9-amine, and 8.2 g of 4,6-dichloropyrimidine, and the mixture was heated to 100° C. and stirred for eleven hours. The mixture was then poured into water and extracted with toluene. The organic layer was washed with water and dried (sat. NaCl, anhydrous MgSO4).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04983608 |
|---|
| Source dataset | uspto-grants-1991_01 |
|---|
| ORD ID | ord-a7388f9ef5eb4387b6e71156e2442219 |
|---|
| Source note | uspto-grants-1991_01 |
|---|
