HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indan-5-amine → HCID 15053109, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indan-5-amine | HCID 90496 | — |
| Reactant | 3-Fluoro-4-nitropyridin-1-ium-1-olate | HCID 594028 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 15053109 | HCID 15053109 | 93.3% |
Reaction Steps
A solution of 3-fluoro-4-nitropyridine-1-oxide (12 g) and indan-5-amine (10 g) in 200 ml ethanol was stirred at reflux for two hours, and thereafter cooled, diluted with ether and filtered to give 19 g solid, m.p. 195°. Four grams were recrystallized from ethanol to give 2.6 g crystals, m.p. 194°-195°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04983615 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-c84cdbccf2474d7ba5bdd9c9b45ddad7 |
| Source note | uspto-grants-1991_01 |