2,2'-Dithiobis(5-chloroaniline) → N,N'-[dithiobis(5-chloro-2,1-phenylene)]bis(1-benzofuran-2-sulfonamide)

HRID 70351Notes

Reaction equation

HRID 70351 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([S:9][S:10][C:11]2[CH:17]=[CH:16][C:15]([Cl:18])=[CH:14][C:12]=2[NH2:13])=[C:6]([CH:8]=1)[NH2:7].[O:19]1[C:23]2[CH:24]=[CH:25][CH:26]=[CH:27][C:22]=2[CH:21]=[C:20]1[S:28](Cl)(=[O:30])=[O:29]>>[Cl:18][C:15]1[CH:16]=[CH:17][C:11]([S:10][S:9][C:5]2[CH:4]=[CH:3][C:2]([Cl:1])=[CH:8][C:6]=2[NH:7][S:28]([C:20]2[O:19][C:23]3[CH:24]=[CH:25][CH:26]=[CH:27][C:22]=3[CH:21]=2)(=[O:29])=[O:30])=[C:12]([NH:13][S:28]([C:20]2[O:19][C:23]3[CH:24]=[CH:25][CH:26]=[CH:27][C:22]=3[CH:21]=2)(=[O:30])=[O:29])[CH:14]=1

Participants

3

Reactant 2

HCID 947422,2'-Dithiobis(5-chloroaniline)HCID 27951721-Benzofuran-2-sulfonyl chloride

Product 1

HCID 86667125N,N'-[dithiobis(5-chloro-2,1-phenylene)]bis(1-benzofuran-2-sulfonamide)

Procedure

Following General Procedure F, the title compound was prepared from 2,2′-dithiobis(5-chloroaniline) and 1-benzofuran-2-sulfonyl chloride.

Sources & evidence

ORD record
ord-670df2061bba472a81a14e3cc70b3c4d
Source dataset
uspto-grants-2014_09
Patent number
US08822530B2

Reaction notes

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