Styrene → 21282-96-2

Participants

Reaction Steps

Eighty four parts of diketene was added dropwise to solution containing 116 parts of 2-hydroxyethyl acrylate, 0.03 parts of diazabicyclooctane and 200 parts of styrene at 70° to 80° C. and mixed for one hour. The obtained solution was condensed at a reduced pressure to obtain 200 parts of acetoacetoxyethyl acrylate. The compound was reacted with 68 parts of aluminum isopropoxyde as generally described in Production Example 27 to obtain a ligand compound D-V of 209 parts (IR absorption 1606 cm-1 and 1525 cm-1 which are derived from chelating).

Provenance & Evidence