HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 1-Octyloxy-4-methacryloyloxy-2,2,6,6-tetramethylpiperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | 1-Octyloxy-2,2,6,6-tetramethylpiperidin-4-ol | HCID 11346683 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1-Octyloxy-4-methacryloyloxy-2,2,6,6-tetramethylpiperidine | HCID 21082393 | — |
Reaction Steps
The procedure of Example 3 is repeated using 1-octyloxy-4-hydroxy-2,2,6,6-tetramethylpiperidine, methacryloyl chloride and triethylamine in methylene chloride to afford the title compound as a colorless oil. Analyses by nmr, ir and ms give data consistent with the desired structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04983737 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-5a7735eba50846bb83e46199486f3768 |
| Source note | uspto-grants-1991_01 |