HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-(2-Chloroethoxy)ethoxy)ethanol → 2-{2-[2-(2-Hydroxyethoxy)ethoxy]ethyl}-1H-isoindole-1,3(2H)-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-(2-Chloroethoxy)ethoxy)ethanol | HCID 78871 | — |
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-{2-[2-(2-Hydroxyethoxy)ethoxy]ethyl}-1H-isoindole-1,3(2H)-dione | HCID 11150157 | — |
Reaction Steps
188 g of 2-[2-(2-Chloroethoxy)ethoxy]ethanol and 146 g of potassium phtalimide in 700 ml of dimethylformamide are brought to 95° C. for 17 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04983740 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-72e4280032b94921a26bb358c0c757c5 |
| Source note | uspto-grants-1991_01 |