HuagongsheHuagongshe Chemistry Print Report · For research reference only
(R)-(-)-alpha-methoxyphenylacetic acid → (R)-(-)-2-Methoxy-2-phenylethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (R)-(-)-alpha-methoxyphenylacetic acid | HCID 2724294 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | (R)-(-)-2-Methoxy-2-phenylethanol | HCID 6950345 | — |
Reaction Steps
72 g of (R)-2-phenyl-2-methoxyacetic acid (prepared according to the method described in J. Chem. Soc., 1962, p. 1519), are reduced with 16.5 g of lithium aluminum hydride in 300 ml of tetrahydrofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04983740 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-5b5d0c7a647c478a84be44df297594cd |
| Source note | uspto-grants-1991_01 |