HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → 2-(Benzylthio)-5-chloroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Amino-4-chlorobenzenethiol | HCID 12000 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-(Benzylthio)-5-chloroaniline | HCID 12618210 | 112.3% |
Reaction Steps
Following General Procedure A, the title compound (819 mg, 100%) was prepared from 2-amino-4-chlorobenzenethiol (700 mg, 4.39 mmol), (bromomethyl)benzene (560 mg, 2.92 mmol), K2CO3 (2.0 g, 14.62 mmol) in DMF (20 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08822530B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-7ee4a1b821d74436ba718f4f44c834a8 |
| Source note | uspto-grants-2014_09 |