Sulfanilamide → HCID 15712773, compound

HRID 703773Notes

Reaction equation

HRID 703773 reaction equation
[C:1]([N:11]1[CH2:18][CH2:17][CH2:16][CH:12]1[C:13]([OH:15])=O)([O:3][CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)=[O:2].[NH2:19][C:20]1[CH:25]=[CH:24][C:23]([S:26]([NH2:29])(=[O:28])=[O:27])=[CH:22][CH:21]=1>>[C:1]([N:11]1[CH2:18][CH2:17][CH2:16][CH:12]1[C:13]([NH:19][C:20]1[CH:25]=[CH:24][C:23]([S:26]([NH2:29])(=[O:27])=[O:28])=[CH:22][CH:21]=1)=[O:15])([O:3][CH2:4][C:5]1[CH:6]=[CH:7][CH:8]=[CH:9][CH:10]=1)=[O:2]

Participants

3

Reactant 2

HCID 5333SulfanilamideHCID 232388N-(Carbobenzyloxy)-DL-proline

Product 1

HCID 15712773HCID 15712773, compound

Procedure

The reaction and recovery procedures of Example I are observed while reacting N-carbobenzyloxy-DL-proline with 4-aminobenzenesulfonamide to yield the desired product, 4-(N-carbobenzyloxy-DL-prolylamino)benzenesulfonamide, having a mp. of 144°-150° C.

Workup

  1. customThe reaction and recovery procedures of Example I

Sources & evidence

ORD record
ord-268840fffd234400b451506e7bbf004d
Source dataset
uspto-grants-1991_01
Patent number
US04985417

Reaction notes

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