HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 16558688, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 22351715 | HCID 22351715 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 16558688 | HCID 16558688 | 82% |
Reaction Steps
Following General Procedure A, the title compound (580 mg, 82%) was prepared from 4-mercapto-3-nitrobenzonitrile (473 mg, 2.63 mmol), (bromomethyl)benzene (449 mg, 2.63 mmol), K2CO3 (1.81 g, 13.14 mmol) in DMF (10 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08822530B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-d53776e418ab49ab902611779166cbdd |
| Source note | uspto-grants-2014_09 |