Aniline → 3-Methyl-N-phenylbut-2-enamide

HRID 703926Notes

Reaction equation

HRID 703926 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:8][C:9]([CH3:14])=[CH:10][C:11](Cl)=[O:12]>>[C:2]1([NH:1][C:11](=[O:12])[CH:10]=[C:9]([CH3:14])[CH3:8])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 6115AnilineHCID 1023943-Methyl-2-butenoyl chloride

Product 1

HCID 123870223-Methyl-N-phenylbut-2-enamideYield 86%

Procedure

This is prepared analogously to a) from aniline and 3,3-dimethylacryloyl chloride. Yield 86% of theory; m.p. 124°-126° C.

Sources & evidence

ORD record
ord-4ffb8aaac5c0483494f7eda21becb2fb
Source dataset
uspto-grants-1991_01
Patent number
US04985448

Reaction notes

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