HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → 5-n-Butyl-2,2-dimethyl 1,3 benzodioxol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | 4-Butylbenzene-1,2-diol | HCID 14368879 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 5-n-Butyl-2,2-dimethyl 1,3 benzodioxol | HCID 15165617 | — |
Reaction Steps
The same procedures as described in Example 10 were carried out by using 4.16 g (25 mM) of 4-n-butylcatechol, 15 ml of acetone, 30 mg of p-toluenesulfonic acid monohydrate and 7 ml of benzene. 5-n-Butyl-2,2-dimethyl-1,3 -benzodioxol was obtained in the yield of 4.74 g (23 mM) as colorless transparent liquid having a boiling point of 74°-75° C./1 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04985458 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-061af798e7ac4cabb9d3d68a3430e5a2 |
| Source note | uspto-grants-1991_01 |