HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 15165618, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | 4-(2-Methylpropyl)-1,2-benzenediol | HCID 14372665 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15165618 | HCID 15165618 | — |
Reaction Steps
The same procedures as described in Example 10 were carried out by using 4.16 g (25 mM) of 4-isobutylcatechol, 15 ml of acetone, 30 mg of p-toluenesulfonic acid monohydrate and 15 ml of toluene. 5-Isobutyl-2,2-dimethyl-1,3-benzodioxol was obtained in the yield of 4.69 g (23 mM) as colorless transparent liquid having a boiling point of 79°-83° C./2 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04985458 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-3d52b60b84634b9dbf0d80c7750c40d2 |
| Source note | uspto-grants-1991_01 |