Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 704054Generated: October 26, 2026

4-Methoxyphenol → Ethyl carbamate;bis(2-methylprop-2-enoic acid)

https://huagongshe.com/reaction/704054

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-MethoxyphenolHCID 9015—
Reactant2-Hydroxypropyl methacrylateHCID 13539—
Reactant1,3-Bis(1-isocyanato-1-methylethyl)benzeneHCID 17719—
ReactantHCID 178443304HCID 178443304—
ProductEthyl carbamate;bis(2-methylprop-2-enoic acid)HCID 21885196—

Reaction Conditions

Temperature60 °C

Reaction Steps

244 Parts of m-tetramethylxylene diisocyanate and 0.3 part of hydroquinone monomethyl ether were charged in a three necked flask and thereto was added dropwise a mixture of 302 parts of 2-hydroxypropyl methacrylate and 0.3 part of n-butyl tin dilaurate over a period of 3 hours with stirring at 60° C. After completion of the addition, reaction was allowed to proceed for 8 hours at 70° C. to obtain urethane dimethacrylate UDM1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04985472
Source datasetuspto-grants-1991_01
ORD IDord-67ace28a40ae4701904488b981fbeec4
Source noteuspto-grants-1991_01