Diethyl butylmalonate → HCID 20075584, compound

HRID 704142Notes

Reaction equation

[OH:1][CH2:2][C:3]([CH2:10][OH:11])([CH2:6][CH:7]([CH3:9])C)[CH2:4][SH:5].[CH2:12](C(C(OCC)=O)C(OCC)=O)CCC>>[OH:11][CH2:10][C:3]([CH2:2][OH:1])([CH2:6][CH2:7][CH2:9][CH3:12])[CH2:4][SH:5]

Participants

Reactant 2

HCID 67244Diethyl butylmalonate

HCID 20075559HCID 20075559, compound

Product 1

HCID 20075584HCID 20075584, compound

Procedure

2,2-di-hydroxymethyl-hexan-1-thiol was prepared in an analogous manner to 2,2-di-hydroxymethyl-4-methyl-pentan-1-thiol starting from diethyl n-butylmalonate.

Sources & evidence

ORD record: ord-f9d375e7a3e741d18432be7a8d79606c
Source dataset: uspto-grants-1991_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04985582

Reaction notes

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