2-Benzyloxymethyl-2-n-propyl-propan-1,3-diol → 2-Hydroxymethyl-2-n-propylpropan-1,3-dithiol

HRID 704148Notes

Reaction equation

HRID 704148 reaction equation
[CH2:1]([C:5]([CH2:10][OH:11])([CH2:8][SH:9])[CH2:6][SH:7])[CH:2](C)[CH3:3].C(OCC(CCC)(CO)CO)C1C=CC=CC=1>>[OH:11][CH2:10][C:5]([CH2:1][CH2:2][CH3:3])([CH2:8][SH:9])[CH2:6][SH:7]

Participants

3

Reactant 2

HCID 200755732-Benzyloxymethyl-2-n-propyl-propan-1,3-diolHCID 231725902-i-Butyl-2-hydroxymethylpropan-1,3-dithiol

Product 1

HCID 193733022-Hydroxymethyl-2-n-propylpropan-1,3-dithiol

Procedure

2-hydroxymethyl-2-n-propyl-propan-1,3-dithiol was prepared in an analogous manner to 2-i-butyl-2-hydroxymethyl-propan-1,3-dithiol starting from 2-benzyloxymethyl-2-n-propyl-propan-1,3-diol.

Sources & evidence

ORD record
ord-26ae4a4979ce4c65ad43e8539e738f02
Source dataset
uspto-grants-1991_01
Patent number
US04985582

Reaction notes

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