1-Bromo-4-(trimethoxymethyl)benzene → HCID 20075564, compound
Reaction equation
CO[C:3]([O:13][CH3:14])(OC)[C:4]1[CH:9]=[CH:8][C:7]([Br:10])=[CH:6][CH:5]=1.OC[C:17]([CH2:22][CH2:23][CH3:24])([CH2:20][SH:21])[CH2:18][SH:19]>>[Br:10][C:7]1[CH:6]=[CH:5][C:4]([C:3]23[S:21][CH2:20][C:17]([CH2:22][CH2:23][CH3:24])([CH2:18][S:19]2)[CH2:14][O:13]3)=[CH:9][CH:8]=1Participants
3
Procedure
1-(4-Bromophenyl)-4-n-propyl-2-oxa-6,7-dithiabicyclo[2,2,2]octane was prepared from trimethyl 4-bromo-orthobenzoate and 2-hydroxymethyl-2-n-propyl-propan-1,3-dithiol.
Sources & evidence
- ORD record
- ord-5940ba2ce2c044c5b3119793df9b2a09
- Source dataset
- uspto-grants-1991_01
- Patent number
- US04985582
Reaction notes
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