Methyl Stearate → HCID 21958155, compound

Participants

Reaction Steps

In a 250-ml three-necked flask equipped with a KPG stirrer, internal thermometer, and short helical glass column followed by a Liebig condenser, 74.6 g methyl octadecanoate and 64.2 g 1,2,2,6,6-pentamethyl-4-piperidinol were heated 6 hr at 200° C. in the presence of 1 g tetraisopropyl titanate, with a gentle nitrogen stream being passed through the reaction mixture A 28 g amount of a distillate was obtained.

Provenance & Evidence