HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 14774041, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ethyl 2-thiopheneglyoxylate | HCID 77693 | — |
| Product | HCID 14774041 | HCID 14774041 | — |
Reaction Steps
13.6 g of ammonia are passed into a cooled solution of 73.6 g of ethyl 2-thienylglyoxylate, and the resulting mixture is stirred at room temperature for 2 h. The solvent is stripped off in vacuo, and the residue is recrystallized from water:ethanol (80:20).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04987134 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-996d1e0919d649b3a051954f84c4602f |
| Source note | uspto-grants-1991_01 |