HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 43250974, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Amino-4-chlorobenzenethiol | HCID 12000 | — |
| Reactant | Methyl 3-(bromomethyl)benzoate | HCID 517981 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 43250974 | HCID 43250974 | 42% |
Reaction Steps
Following General Procedure A, the title compound (1.4 g, 42%) was prepared from 2-amino-4-chlorobenzenethiol (1.7 g, 10.90 mmol), methyl 3-(bromomethyl)benzoate (2.5 g, 10.90 mmol) and K2CO3 (7.5 g, 54.50 mmol) in DMF (30 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08822530B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-7b39c488c98246a79168b6ea79c7509a |
| Source note | uspto-grants-2014_09 |