HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → Methyl 2-(((2-amino-4-methylphenyl)thio)methyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | HCID 86690996 | HCID 86690996 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 2-(((2-amino-4-methylphenyl)thio)methyl)benzoate | HCID 82976265 | 85% |
Reaction Steps
Following General Procedure L, the title compound (567 mg, 85%) was prepared from methyl 2-(((4-methyl-2-nitrophenyl)thio)methyl)benzoate (741 mg, 2.34 mmol), Zn (3.7 g, 58.44 mmol) and saturated aqueous NH4Cl (1 ml) in MeOH (20 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08822530B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-8dd9d80091d2474c98d9376f35926bf2 |
| Source note | uspto-grants-2014_09 |