HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Diphenylmethoxy-1-(2,2-dimethoxyethyl)-6-hydroxymethyl-4-pyridone → 3-Diphenylmethoxy-1-(2,2-dimethoxyethyl)-6-formyl-4pyridone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Diphenylmethoxy-1-(2,2-dimethoxyethyl)-6-hydroxymethyl-4-pyridone | HCID 15058192 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Product | 3-Diphenylmethoxy-1-(2,2-dimethoxyethyl)-6-formyl-4pyridone | HCID 15058193 | — |
Reaction Steps
Starting from 2.052 g of 3-diphenylmethoxy-1-(2,2-dimethoxyethyl)-6-hydroxymethyl-4-pyridone and 12.0 g of manganese dioxide, the title compound is obtained in the same manner as in Synthesis Example 2 as colorless crystal in a yield of 1.582 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04988686 |
| Source dataset | uspto-grants-1991_01 |
| ORD ID | ord-b797dd52577f49a0970fc5973d437d1e |
| Source note | uspto-grants-1991_01 |