Diallyl ether → HCID 67925638, compound

Participants

Reaction Steps

140 grams of the diallyl ether of indane bisphenol was placed into a one liter round bottom flask containing a magnetic stir bar and dissolved in 210 grams of 2-(2-ethoxyethoxy) ethanol. The solution was deoxygenated by bubbling dry argon gas through the solution for 15 minutes, and then a reflux condenser was attached. The solution was refluxed for 6 hours under an inert atmosphere. The solvent was removed by vacuum distillation between 60° and 62° C., and the product was collected between 210° and 214° C. as a light yellow, viscous liquid (13.3 Pa). Diallyl indane bisphenol was so viscous that the condenser on the still has to be heated with a hot air gun so that the product could flow into the collection flask; 110 grams of diallyl indane bisphenol were isolated (75% yield overall).

Provenance & Evidence