HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexane → Chloramben-methyl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexane | HCID 8058 | — |
| Reactant | Chloramben | HCID 8630 | — |
| Reactant | Trimethylsilyldiazomethane | HCID 167693 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Chloramben-methyl | HCID 23714 | — |
Reaction Steps
206 mg (1.0 mmol) of 2,5-Dichloro-3-aminobenzoic acid was dissolved in 4 mL of acetone. 0.7 mL (1.4 mmol) of A hexane solution of 2.0M trimethylsilyldiazomethane was added thereto and stirred at room temperature for 1.5 hours. A solvent was removed to obtain methyl 2,5-dichloro-3-aminobenzoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09174932B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-1cfcecd5fdcd4c12abcdfff6406355ba |
| Source note | uspto-grants-2015_11 |